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The temperature of the ion source was set at 280 C, and the ionization voltage was 70 eV

To interpret the binding isotope effects quantitatively, we performed ab initio calculations that were then used to calculate binding isotope effects.[75, 81] The C-H bond of a model 5-deoxypyridoxal-Ala imine was incrementally lengthened and held fixed while the geometry of the remaining atoms was optimized