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The mass spectrum with positive ionization mode for complex 2 after 1 min of incubation showed two signals of the iron(III) complex at m/z = 254 and at m/z = 376, corresponding to the [M L] + and [M + Na] + species

There was a significant interaction with smoking status in the uni-variable model as well as model b ( p = 0.074 and p = 0.079, respectively), but not with sex ( p = 0.462 and p = 0.606, respectively) (Table 2)

Such sites include the synovium and cartilage of peripheral joints (particularly occurring first in the more distal, cooler joints), the olecranon bursa and the helix of the ear

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